深度分辨聚合物固化过程监测:对比研究与自适应帧间距优化方法
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1.广东工业大学自动化学院广州510006; 2.广东工业大学智能检测与制造物联教育部重点实验室广州510006; 3.广东工业大学广东省智能系统与优化集成重点实验室广州510006

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TH691.9

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国家自然科学基金(62475048,62571145)、广东省自然科学基金(2024A1515010230)项目资助


Deep-resolution monitoring of polymer curing process: Comparative study and adaptive inter-frame spacing optimization method
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1.School of Automation, Guangdong University of Technology, Guangzhou 510006, China; 2.Key Laboratory of Intelligent Detection and Manufacturing of IoT of the Ministry of Education, Guangdong University of Technology, Guangzhou 510006, China; 3.Guangdong Province Key Laboratory of Intelligent System and Optimization Integration, Guangdong University of Technology, Guangzhou 510006, China

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    摘要:

    深度分辨的固化过程可视化监测方法对深入理解聚合物固化动力学、优化固化工艺具有极其重要的意义。近年来,国际上相继发展出基于数字图像相关(digital image correlation, DIC)和相位敏感探测(phase sensitive detection, PhS)方法的两类功能型光学相干层析成像技术(optical coherence tomography, OCT),这两种技术凭借非接触、高分辨率、实时监测的优势,已成为聚合物固化监测的有效手段,但目前研究还存在两方面局限:一方面,缺乏两种方法在实际场景下的系统量化对比;另一方面PhS-OCT受2π相位模糊效应制约,难以兼顾大形变条件下的监测需求。针对上述问题,量化对比了DIC-OCT与PhS-OCT在测量灵敏度、范围及抗噪声能力方面的差异,明确两种技术的适用边界。在此基础上,创新性提出基于相位梯度的自适应帧间距调节方法,通过构建“相位梯度-信噪比耦合”的动态调节机制,动态调整监测帧间距,实现量程拓展与累积误差抑制的协同优化。为验证所提方法的有效性与实用性,分别开展了双层复合树脂固化实验与牙齿修复模拟实验:在双层树脂实验中,成功将PhS-OCT的监测量程从-12.21 mε拓展至-22.15 mε,同时计算效率较传统增量法提升24倍;在牙釉质高反射散斑的复杂噪声环境中,DIC-OCT应变计算失效区域占比达16.8%,而所提方法依托强抗噪性与动态量程拓展能力,实现了树脂固化全过程的可靠监测。该方法与PhS-OCT深度融合后,可实现聚合物固化过程的高精度、大形变、全场动态监测。

    Abstract:

    Visualization monitoring methods with high depth resolution for the curing process are of great significance for in-depth understanding of polymer curing kinetics and optimizing curing processes. In recent years, two types of functional optical coherence tomography (OCT) techniques based on digital image correlation (DIC) and phase-sensitive detection (PhS) have been developed internationally. With the advantages of non-contact, high-resolution and real-time monitoring, these techniques have become effective means for polymer curing monitoring. However, current research still presents two main limitations. First, there is a lack of systematic quantitative comparison between the two methods in practical scenarios. Second, PhS-OCT is restricted by the 2π phase wrapping effect, making it difficult to meet the monitoring requirements under large deformation conditions. To address the above problems, this study quantitatively compares the differences between DIC-OCT and PhS-OCT in measurement sensitivity, range and noise immunity, and clarifies the applicable boundaries of the two techniques. On this basis, an adaptive frame interval adjustment method based on phase gradient is innovatively proposed. By constructing a dynamic regulation mechanism of "phase gradient-signal-to-noise ratio coupling", the monitoring frame interval is dynamically adjusted to achieve collaborative optimization of measurement range expansion and cumulative error suppression. To verify the effectiveness and practicability of the proposed method, curing experiments of double-layer composite resin and simulated dental restoration experiments are carried out respectively. In the double-layer resin experiment, the monitoring range of PhS-OCT is successfully expanded from -12.21 mε to -22.15 mε, and the computational efficiency is improved by 24 times compared with the traditional incremental method. In the complex noise environment of enamel with high-reflection speckles, the proportion of invalid strain calculation regions of DIC-OCT reaches 16.8%, while the proposed method achieves reliable monitoring of the whole resin curing process relying on strong noise immunity and dynamic range expansion capability. After deep integration with PhS-OCT, this method realizes high-precision, large-deformation and full-field dynamic monitoring of polymer curing process.

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杨康,白玉磊,董博.深度分辨聚合物固化过程监测:对比研究与自适应帧间距优化方法[J].仪器仪表学报,2026,47(3):83-93

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  • 在线发布日期: 2026-05-22
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